Visit chemicalbook to find more saccharin sodium (128-44-9) information like chemical properties,structure,melting point,boiling point,density,molecular formula,molecular weight, physical properties,toxicity information,customs codes. In this experiment, we alkylate sodium saccharin to n-ethylsaccharin with iodoethane in an aprotic solvent n,n dimethylformamide nucleophiles in this experiment will react better in an aprotic solvent. Created date: 1/6/2006 11:58:20 am. Preparation of n-ethyl saccharin s n o o o saccharin s n o o o na sodium saccharin –add sodium saccharin –mixture needs to be warmed for 20 min (hot plate.
Operational organic chemistry : a problem-solving approach to the laboratory course reaction of iodoethane with sodium saccharin, an ambident nucleophile. To determine the major product of the reaction between sodium saccharin and iodoethane sodium saccharin, iodoethane, dmf, deuterochloroform. Reaction of iodoethane with sodium saccharin, an ambident nucleophile.
You will use the sodium salt of saccharin as a nucleophile to displace the iodide in iodoethane to produce ethyl saccharin documents and settingssteve murovmy. Fly lab report p saccharin we use is actually the sodium salt of saccharin, and they reject salt solutions overall.
introduction the purpose to of this experiment is to carry out the alkylation of sodium saccharin with iodo-ethane and analyze the product mixture to determine the structure of the major product. Organic chemistry i laboratory ambident nucleophiles:1 experiment 8 reaction of sodium saccharin with iodoethane week 8 background reading zubrick, j w the organic chem lab survival manual, 4th edition, wiley & sons, inc,.
Is the reaction of iodoethane with sodium saccharin a sn1 or sn2 reaction explain why.
Perception of different sugars by the sweetener people use is actually the sodium salt of 1989), flies taste the sodium and so reject saccharin as a salt. Saccharin alkylation: o vs n substitution fred h greenberg j chem educ, 1990, 67 (7), p 611 doi: 101021/ed067p611 publication date: july 1990. Title: reaction of iodoethane with sodium saccharin- ambient nucleophile dates performed: february 21 + 28, 2013 date submitted: march 14, 2013 abstract: the product ratio of n-ethylsaccharin to o-ethylsaccharin that occurred due to alkylation with iodoethane at 80 oc was determined to be 815% to 185%, respectively, based on an analysis of the 1h nmr spectrum that was collected. P 1 1 1 0 he alth fire re activity pe rs onal prote ction 1 1 0 e material safety data sheet sodium saccharin dihydrate msds section 1: chemical product and company identification.Download